Investigation of Microstructural Evolution of Gas-assisted Metal Injection Molded and Sintered Mg-0.5Ca Alloy
Abstract
In this study, Mg-0.5Ca alloy was produced in a newly designed unit during the metal injection molding process. 40μmD90 Mg powder and 500nmD90 Ca powder were used in accordance with injection molding and powder sintering rules. In the injection phase, Polyethylene-glycol (PEG) and Poly-methyl-methacrylate (PMMA) and stearic acid (SA) polymers act as binders and lubricants. In the experimental phase, X-ray Diffractometer (XRD), Thermal Gravimetric Analyze (TGA), Scanning Electron Microscope (SEM) equipped with Energy Dispersive Spectroscopy Mapping (EDS and MAP), and Vickers microhardness (HV) examinations were performed. The samples produced were subjected to the sintering process at different temperatures and times. Conventional powder sinter stages point, neck, and joining structures were obtained at different temperatures and durations. As a result, it was determined that Mg-0.5Ca alloy reached a metallic form with the specified polymer structure only at 600oC temperature and after 5 h sintering. Grain boundaries were formed in the sintered sample and the presence of the Mg2Ca phase was observed. The hardness of the metallic structure obtained was measured as 49.9 HV0.1 on average.
Copyright
Authors retain copyright of the published article and have the right to use the article in the ways permitted to third parties under the Creative Commons Attribution 4.0 International license. Full bibliographic information (authors, article title, journal title, volume, issue, pages) about the original publication must be provided and a link must be made to the article's DOI. This license allows to copy and redistribute the material in any medium or format, remix, transform, and build upon it for any purpose, even commercially, as long as appropriate credit is given to the original author(s), a link to the license is provided and it is indicated if changes were made.